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An ice-cold CH 2 Cl 2 solution of carbonyl diimidazole (0.63 g, 3.84 mmol) was stirred under argon for 5 min before being added via cannula to a CH 2 Cl 2 solution of 11 (1.00 g, 3.49 mmol) and 0.77 mL of N-methylmorpholine (6.99 mmol) over 20 min
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Concentration:10mg
Feb 1997;99(2):239-244
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